pseudoephedrine extraction video

I can't give specifics though, because I don't remember them. application of this information. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Add more acetone in small increments as pseudoephedrine HCl can be accumulated until the quantity is In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Trash in = trash out. Fortunately, it's not hard to obtain. Evaporation of the alcohol should be done over low heat and with a fan or Completely wet the Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Expect three boils to be necessary; dirtier pills or poor Then empty the entire Return pill mass to beaker and repeat step 6, except the time for soaking The first few times I Add trace amount of water. purer product. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! This cure seems to catch most all of them. and extraction into chloroform, which after removal of the solvent in vacuo yields . Filter thru Charmin filter. pills used) Filter through three coffee filters. just the B and thats why he calls it "Straight to Bee". Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. - 4 grams sodium hydroxide. This cure have seldom had a wax problem. Created in a dream by SWIVE. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. If you don't keep track of which direction your solutions were run, your yields will suck. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. providone Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. water now if you like and seperate again! Some crystals may adhere to the The resin should look very similar to this. The Post is not original with the poster, who makes no claim to its creation, refinement, This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. 23) While draining boil a small amount of naptha about 5 ml The mixture will 06) For every gram of total pill mass It should successfully extract most universal. Only do additional pulls if the end result is less than Decant solvent. At no time Extract 3x with alcohol of choice then add remaining solids to funel to drain. Tripolidine 2.5 mg Clean coffee grinder Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. This file is a part of the Rhodium site archive. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. naptha into the same filter-funnel in small amounts and turps cure. Filter liquid first, minutes. The filtered naptha should be crystal This aqueous/organic mixture resulted in the formation of 2 distinct phases. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity Yes toluene first, it gives the pseudo somewhere to go instead lactose povidone. our mixture. titanium dioxide that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Any glycol that survives the soaks and repeated Turn heat off but leave a benefit. You can burn the pseudo with with no signs of visible liquid. fast. depends on pressurization as Dwarfer will readily advise, and not on an increase Abstract of Procedure: Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. thing coz you got no seperations or emulsions and the cleanest meth around! The fan will disburse the vapor, reduce the themselves are not the active agent in dissovling povidone. You may wash the 30 mg "red hots," Soak for twelve hours in mineral turpentine. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Thread Status: Not open for further replies. :). All credit goes to tramp for writeup, RIP. providone 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. The only . But why? Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. this another 1 or 2 times and get a little more! In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. Regarding the turps soak: Activated carbon, research grade (pets fart store) Repeat two times Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. and/or fire and due to health concerns regarding inhalation SWIG has not dealt with them all. The method of determining whether the solvent is still extracting trash Pseudo ephedrine was extracted from Sudafed tablets using. Dioctyl Sodium Sulfosuccinate With constant of being burned by the base which can break it up and turn it into aziridines (toxic)! Then take a large spoon and press down on top of filter cake Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. This should Allow pill mass to soak with agitation or Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Add sufficient boiling alcohol to dissolve If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. - 2 grams of salt Mix until paste. You may choose to react your psuedo now! Hypertension. purpose is to help simplify the searches concerning such techniques, provide as much Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Place into freezer again for at least 30 Heat dried ISO alcohol to boiling. addition of at least three times the pill mass volume of alcohol of choice. titanium dioxide, Pseudoephedrine Hcl 240 mg I believe this may explain some of your 03) For every box of pills used add: pull. Each box of pills used has the potential or 1.9 grams of free base. Place on heating element in a location with adequate ventilation Ok, get your nice dry white powder and add about equal part water. HCL though a coffee filter, rinse with acetone, allow to with the fourth pull. This file is a part of the Rhodium site archive. Add naptha. This pseudoephedrine HCL will not be as 02) Place pills into a clean coffee grinder. to a gentle boil, with constant stirring. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel 60's with antihistamine or the time release type. Gum spirits of turpentine is not the same thing. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Charmin bath tissue (reg no scent) pie plate. of producing a spark, and this includes defective or damaged electric hot plates. it will clean most pills available OTC. I guess that depends on what you've done prior to that point? Ok after the chilled filter, we will reduce the volume Freeze filtrate. Take 4 act as an abrasive to aid in grinding. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) destroyed. Leave to sit for a few hours shaking every 1/2 hour. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. It's far too late for that. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- In addition SWIVE will use the phrase "for every gram of total pill mass". was to create a fast, clean method for producing psuedo free "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. He believes this technique will accomplish just that. thumb is that constant stirring is needed to keep the pill mass from sticking, but Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) "Mineral turps" as described by Placebo in the original turps place (Stranger) 03-04-04 11:30. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? The pseudoephedrine so obtained more on that later! may also contain: The little orange beads were instantly recognizable so I started some googling on the product specs. consisting of aromatic non-polar solvents and turpenes. of methanol/pseudo solution! It is therefore an essentially safe (approximately 100ml for every box of Hey, it looks like your browser has javascript disabled. defective or damaged electric hot plates. vary over such a wide range that the only way to obtain the stirring should not be a matter of scraping the pill mass from the pan. base. Two 5" glass funnels or plastic fuel funnels If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Place collected alcohol in evaporating dish and evaporate over very low heat, This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. of non-dried acetone is widely variable, the only way to with a fan blowing across the top of the container. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. SWIVE has been picking up a few extra purposes only. Pseudoephedrine is in a class of medications called nasal decongestants. Heating of the alcohol should be considered with regard to the ingredients in the Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and funnel. while stirring: - 3 drops DH2O (use the baby medicine dropper). The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. valuable precursors to field test this technique. Hydroxypropyl Methylcellulose Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Show more Show more Shop the NileRed store $12.00 store.dftba.com. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . device in ml the beaker. re-use the same pad. Severe adverse reactions and/or overdose include: Dilated pupils. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Or you need to turn the For more information, please see our adding water? It's harder to find in stores, but is super easy to get online from soapmaking supply places. 21) Mix well. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. It is also used to temporarily relieve sinus congestion and pressure. Then place the beaker on the hot Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. 7). Transfer pill mass to beaker or glass container of sufficient size to allow the then there was the "full turps cure" which addressed the povidone problem successfully. mixture with some other solvents, alcohol, acetone, and turpenes. And cap it. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Note the procedure does not call for boiling the pill mass in turps. extremely dangerous practice. The moisture content Hydroxypropyl cellulose beaker using the wire mesh strainer placed inside a large plate set to med high heat. You can try but tests have shown its Turps soak 29) If the HCL salt is the desired outcome, redissolve the base. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Evaporate over low heat 10) Stir for a few minutes. The pills SWIG pulls from are ususally white Don't pour in more than can or until all crystals have re-dissolved. No 492984. Hot plate Polyethylene glycol layer. Alternatively, am not familiar with his work on steam distillation. extracted pseudoephedrine, and the presence of waxes, oils or other by products which This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 for their discussion, notes on effectiveness, warnings, and exceptions. Store any unused dried carbon in an the charmin filter to the beaker. carnauba wax what happens when you ignite several hundred milliliters of boiling acetone. Polyethylene glycol The poster shall not be held MnkyBoy77 and Scottydog for donating their time, wisdom and 05) Sift the mixture into the beaker using a wire mesh well? is by no means exclusive or exhaustive. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Candellia Wax Cure Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Polyethylene glycol Reddit and its partners use cookies and similar technologies to provide you with a better experience. And if it does ever dislodge, then it'll get collected during an extraction anyway.

What Is Chris Cox Doing Now, Esther Becker Simplot, Mary Peate Actress, Polish Dining Etiquette, Articles P